Hot-press consolidation and tensile strength characterization of mechanically alloyed nanostructured Fe-Al and Fe-C powder
- U. of CA-Davis
Previous studies of nanostructured materials have typically concentrated on characterization of microscopic properties, principally because of the inability to produce samples of sufficient size to determine macroscopic properties. In this study consolidation of mechanically alloyed Fe-AI and Fe-C powders was accomplished by hot-pressing. Microstructure characterizations of both the attritor-processed powder and the consolidated material were determined using X-ray diffraction and SEM. Consolidated samples were of sufficient size (25 mm in diameter and 5-7mm thick) to determine macroscopic properties, most notably tensile strengths. Tensile strength increased with increasing density, reaching a optimal strength of 700 to 900 MPa as the compacts reached full density. The maximum nanostructure tensile strength is consistent with tensile properties of HSLA steels. Compact characteristics (density, hardness, tensile strength) were determined as a function of hot-pressing conditions (processing temperature, time, pressure). During consolidation, Fe-C samples developed second phase spinel and carbide precipitates. During consolidation, Fe-AI samples developed a duplex submicron- and nanograin bcc-Fe microstructures and nanograins of (Fe,Al)3O4. The grains of the consolidated samples were free of grain disorder, e.g., dislocations, twins, etc. With few exceptions, density and grain size increased with increasing hot-press processing time, temperature, and/or pressure.
- Research Organization:
- Albany Research Center (ARC), Albany, OR (United States)
- Sponsoring Organization:
- USDOE - Office of Fossil Energy (FE)
- DOE Contract Number:
- None cited
- OSTI ID:
- 923366
- Report Number(s):
- DOE/ARC-1997-016; TRN: US200804%%1089
- Journal Information:
- NanoStructured Materials, Vol. 9, Issue 1-8; Conference: Third International Conference on Nanostmctured Materials (NANO’96), Kona, HI, July 8-12,1996; ISSN 0965-9773
- Publisher:
- Elsevier
- Country of Publication:
- United States
- Language:
- English
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