A rapidly filled capillary mount for both dry powder and polycrystalline slurry samples
Journal Article
·
· Journal of Applied Crystallography
A method of rapid capillary sample loading of either dry powder or polycrystalline slurry has been developed. By embedding a Millipore filter in a Kapton capillary tube, one can then draw either loose dry powder or polycrystalline slurry into the tube and pack the solid against the filter, creating a dense column of powder suitable for a Debye–Scherrer powder diffraction experiment.
- Research Organization:
- Advanced Photon Source (APS), Argonne National Laboratory (ANL), Argonne, IL (US)
- Sponsoring Organization:
- USDOE
- DOE Contract Number:
- AC02-06CH11357
- OSTI ID:
- 898663
- Journal Information:
- Journal of Applied Crystallography, Journal Name: Journal of Applied Crystallography Journal Issue: 1 Vol. 39; ISSN 0021-8898; ISSN JACGAR
- Publisher:
- International Union of Crystallography
- Country of Publication:
- United States
- Language:
- English
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