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Kinetics of Silica Condensation In Brines

Conference ·
OSTI ID:886858

Homogeneous nucleation and growth of silica from brines supersaturated in silicic acid has been studied over a range of pH (4.5-6.7), temperature (75-105 C), salinity, and silicic acid concentration (700 to 1200 ppm as SiO{sub 2}). The experimental technique involved analyses for molybdate-reactive silicic acid as a function of time after a supersaturated solution of H{sub 4}SiO{sub 4} was prepared by mixing aliquots of a stock silicate solution with buffered brine. The isothermal rate of SiO{sub 2} condensation is a strong function of supersaturation (C/C{sub eq}), pH, and salinity. The overall kinetics follow what is expected from the general theory of phase transitions and are adequately described by the Volmer-Becker-Doring expressions for condensation from solution. At supersaturations less than about 3, an induction or transition time is observed. It amounts to several hundred minutes at supersaturations of about 2.0

Research Organization:
EIC Corporation, Newton, MA
Sponsoring Organization:
USDOE
OSTI ID:
886858
Report Number(s):
COO-2607-4; CONF-760844-4
Country of Publication:
United States
Language:
English

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