Sample introducing apparatus and sample modules for mass spectrometer
- Knoxville, TN
- Kingston, TN
An apparatus for introducing gaseous samples from a wide range of environmental matrices into a mass spectrometer for analysis of the samples is described. Several sample preparing modules including a real-time air monitoring module, a soil/liquid purge module, and a thermal desorption module are individually and rapidly attachable to the sample introducing apparatus for supplying gaseous samples to the mass spectrometer. The sample-introducing apparatus uses a capillary column for conveying the gaseous samples into the mass spectrometer and is provided with an open/split interface in communication with the capillary and a sample archiving port through which at least about 90 percent of the gaseous sample in a mixture with an inert gas that was introduced into the sample introducing apparatus is separated from a minor portion of the mixture entering the capillary discharged from the sample introducing apparatus.
- Research Organization:
- LOCKHEED MARTIN ENRGY SYST INC
- DOE Contract Number:
- AC05-84OR21400
- Assignee:
- Martin Marietta Energy Systems, Inc. (Oak Ridge, TN)
- Patent Number(s):
- US 5272337
- OSTI ID:
- 869087
- Country of Publication:
- United States
- Language:
- English
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Related Subjects
90
air
air monitor
air monitoring
analysis
apparatus
archiving
attachable
capillary
capillary column
column
communication
conveying
described
desorption
discharged
entering
environmental
gas
gaseous
gaseous sample
gaseous samples
including
individually
inert
inert gas
interface
introduced
introducing
liquid
mass
mass spectrometer
matrices
minor
minor portion
mixture
module
modules
monitoring
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percent
portion
preparing
provided
purge
range
rapidly
real-time
real-time air
sample
sample-introducing
samples
separated
soil
spectrometer
split
split interface
supplying
supplying gas
thermal
thermal desorption
time air
wide
wide range