Process for producing low-sulfur boiler fuel by hydrotreatment of solvent deashed SRC
Patent
·
OSTI ID:865550
In this invention, a process is disclosed characterized by heating a slurry of coal in the presence of a process-derived recycle solvent and passing same to a dissolver zone, separating the resultant gases and liquid/solid products therefrom, vacuum distilling the liquid/solids products, separating the portions of the liquid/solids vacuum distillation effluent into a solid ash, unconverted coal particles and SRC material having a boiling point above 850.degree. F. and subjecting same to a critical solvent deashing step to provide an ash-free SRC product. The lighter liquid products from the vacuum distillation possess a boiling point below 850.degree. F. and are passed through a distillation tower, from which recycled solvent is recovered in addition to light distillate boiling below 400.degree. F. (overhead). The ash-free SRC product in accompanyment with at least a portion of the process derived solvent is passed in combination to a hydrotreating zone containing a hydrogenation catalyst and in the presence of hydrogen is hydroprocessed to produce a desulfurized and denitrogenized low-sulfur, low-ash boiler fuel and a process derived recycle solvent which is recycled to slurry the coal in the beginning of the process before heating.
- Research Organization:
- International Coal Refining Company, Allentown, PA (United States)
- Sponsoring Organization:
- USDOE
- DOE Contract Number:
- AC05-78OR03054
- Assignee:
- International Coal Refining Company (Allentown, PA)
- Patent Number(s):
- 4,534,847
- Application Number:
- 06/571,311
- OSTI ID:
- 865550
- Country of Publication:
- United States
- Language:
- English
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Related Subjects
/208/
400
850
accompanyment
addition
ash
ash-free
beginning
below
boiler
boiler fuel
boiling
boiling below
catalyst
characterized
coal
coal particle
coal particles
combination
containing
critical
critical solvent
deashed
deashing
degree
denitrogenized
derived
derived solvent
desulfurized
disclosed
disclosed characterized
dissolver
distillate
distillation
distillation tower
distilling
effluent
fuel
gases
heating
hydrogen
hydrogenation
hydrogenation catalyst
hydroprocessed
hydrotreating
hydrotreatment
light
light distillate
lighter
liquid
liquid product
liquid products
low-ash
low-sulfur
material
overhead
particles
passed
passing
portion
portions
possess
presence
process
process derived
process-derived
produce
producing
product
products
provide
recovered
recycle
recycle solvent
recycled
resultant
separating
slurry
solid
solid product
solid products
solids
solvent
solvent deashing
src
src product
step
subjecting
therefrom
tower
unconverted
unconverted coal
vacuum
vacuum distillation
zone
zone containing
400
850
accompanyment
addition
ash
ash-free
beginning
below
boiler
boiler fuel
boiling
boiling below
catalyst
characterized
coal
coal particle
coal particles
combination
containing
critical
critical solvent
deashed
deashing
degree
denitrogenized
derived
derived solvent
desulfurized
disclosed
disclosed characterized
dissolver
distillate
distillation
distillation tower
distilling
effluent
fuel
gases
heating
hydrogen
hydrogenation
hydrogenation catalyst
hydroprocessed
hydrotreating
hydrotreatment
light
light distillate
lighter
liquid
liquid product
liquid products
low-ash
low-sulfur
material
overhead
particles
passed
passing
portion
portions
possess
presence
process
process derived
process-derived
produce
producing
product
products
provide
recovered
recycle
recycle solvent
recycled
resultant
separating
slurry
solid
solid product
solid products
solids
solvent
solvent deashing
src
src product
step
subjecting
therefrom
tower
unconverted
unconverted coal
vacuum
vacuum distillation
zone
zone containing