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Thermal shock resistance ceramic insulator

Patent ·
OSTI ID:863718

Thermal shock resistant cermet insulators containing 0.1-20 volume % metal present as a dispersed phase. The insulators are prepared by a process comprising the steps of (a) providing a first solid phase mixture of a ceramic powder and a metal precursor; (b) heating the first solid phase mixture above the minimum decomposition temperature of the metal precursor for no longer than 30 minutes and to a temperature sufficiently above the decomposition temperature to cause the selective decomposition of the metal precursor to the metal to provide a second solid phase mixture comprising particles of ceramic having discrete metal particles adhering to their surfaces, said metal particles having a mean diameter no more than 1/2 the mean diameter of the ceramic particles, and (c) densifying the second solid phase mixture to provide a cermet insulator having 0.1-20 volume % metal present as a dispersed phase.

Research Organization:
Oak Ridge National Laboratory (ORNL), Oak Ridge, TN
Assignee:
United States of America as represented by United States (Washington, DC)
Patent Number(s):
US 4234338
OSTI ID:
863718
Country of Publication:
United States
Language:
English