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Millimeter-Wave Measurements at 137 GHZ of DWPF Black Frit Glass Flow and Salt Layer Pooling in a Pilot Scale Melter

Conference ·
OSTI ID:826057

Nuclear waste vitrification in joule-heated melters would be greatly facilitated by the availability of on-line monitoring instrumentation for critical process parameters such as viscosity and salt accumulation. A field test of the applicability of millimeter-wave (MMW) technology to providing such tools was carried out on a pilot scale melter (EV-16) at the Clemson Environmental Technology Laboratory. Flow measurements of Defense Waste Processing Facility (DWPF) black frit glass over a temperature (T) range of 800-1150 C and to depths of over 7 inches (17.8 cm) were made with an immersed ceramic waveguide. Pressure induced melt flow inside the waveguide was observed over an average velocity range of 0.1-10 mm/s consistent with a 1/T viscosity scaling. In another test, sodium sulfate salt (NaSO4) was added to the melt to demonstrate salt layer detection. A 30% decrease in MMW melt emissivity was clearly observed as pools of salt formed and flowed under the waveguide.

Research Organization:
Massachusetts Institute of Technology, MA; Pacific Northwest National Lab., Richland, WA; Savannah River Technology Center, Aiken, SC; Clemson University, SC (US)
Sponsoring Organization:
USDOE Office of Science (SC) (US)
OSTI ID:
826057
Country of Publication:
United States
Language:
English