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Title: Microstructure and Pinning Properties of Hexagonal Disc Shaped Single Crystalline MgB2

Technical Report ·
DOI:https://doi.org/10.2172/813043· OSTI ID:813043

We synthesized hexagonal-disc-shaped MgB{sub 2} single crystals under high-pressure conditions and analyzed the microstructure and pinning properties. The lattice constants and the Laue pattern of the crystals from X-ray micro-diffraction showed the crystal symmetry of MgB{sub 2}. A thorough crystallographic mapping within a single crystal showed that the edge and c-axis of hexagonal-disc shape exactly matched the (10-10) and the (0001) directions of the MgB{sub 2} phase. Thus, these well-shaped single crystals may be the best candidates for studying the direction dependences of the physical properties. The magnetization curve and the magnetic hysteresis for these single crystals showed the existence of a wide reversible region and weak pinning properties, which supported our single crystals being very clean.

Research Organization:
SLAC National Accelerator Lab., Menlo Park, CA (United States)
Sponsoring Organization:
USDOE Office of Science (US)
DOE Contract Number:
AC03-76SF00515
OSTI ID:
813043
Report Number(s):
SLAC-PUB-9738; TRN: US200315%%213
Resource Relation:
Other Information: PBD: 30 Apr 2003
Country of Publication:
United States
Language:
English