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High temperature deformation of MgO

Technical Report ·
DOI:https://doi.org/10.2172/7357409· OSTI ID:7357409
The deformation and recovery of both single crystals ((100), (110), (111) and Ni-doped (100)) and fully dense polycrystals (with grain sizes ranging from 4 to 160 ..mu..m) of MgO were studied under compressive stress-strain and creep testing conditions at 1200/sup 0/C (0.48 Tm) and 1400/sup 0/C (0.55 Tm). Emphasis was placed on the aspects relevant to ductility such as recovery contribution and the role of grain boundaries. No polycrystals were harder than a (111) crystal, nor softer than a (100) crystal, which represented dislocation glide on the more difficult and less difficult slip planes, respectively. Plastic anisotropy between these slip planes decreased and polycrystaline ductility increased with decreasing strain rate as well as increasing temperature. Simultaneous activation of all five independent slip systems did not lead to a large ductility. A maximum ductility was observed for the smallest grain size under given testing conditions. In addition to slip on both planes and dislocation-climb-aided accommodation, intergranular separation is suggested as a mode of accommodation, although it was accompanied by weakening effects. Significance of grain boundary nature, per se, was indicated by variability of the mechanical behavior as a function of prior annealing history for the same grain size. (auth)
Research Organization:
California Univ., Berkeley (USA). Lawrence Berkeley Lab.
DOE Contract Number:
W-7405-ENG-48
OSTI ID:
7357409
Report Number(s):
LBL-3979
Country of Publication:
United States
Language:
English