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Radiation decomposition of p-nitroperoxybenzoic acid in solution. [Gamma rays]

Journal Article · · J. Phys. Chem.; (United States)
DOI:https://doi.org/10.1021/j100553a003· OSTI ID:7355040

p-Nitroperoxybenzoic acid is reduced by carboxyl radical anions which arise from the interaction of .OH with formic acid or formate ions at pH greater than 3. The resulting electron adduct of p-nitroperoxybenzoic acid (I) eliminates an .OH radical which subsequently propagates a chain reaction. The inverse square-root law for the dose rate has been confirmed for the chain process. G values greater than 200 were observed for the decomposition of the peroxy acid. An activation energy of 2.7 kcal mol/sup -1/ has been attributed to the elimination of .OH from radical anion I. 2-Hydroxyl-2-propyl radicals, formed through hydrogen abstraction from 2-propanol by .OH, also sustain a chain reaction in solutions of p-nitroperoxybenzoic acid, but the kinetic chain length is considerably reduced in comparison with reactions of carboxyl radical anions.

Research Organization:
East Carolina Univ., Greenville, NC
OSTI ID:
7355040
Journal Information:
J. Phys. Chem.; (United States), Journal Name: J. Phys. Chem.; (United States) Vol. 80:12; ISSN JPCHA
Country of Publication:
United States
Language:
English