Heteronuclear dipolar modulated chemical shift spectra for geometrical information in polycrystalline solids

Journal Article · Sun Nov 14 23:00:00 EST 1976 · J. Chem. Phys.; (United States)

DOI:https://doi.org/10.1063/1.432863· OSTI ID:7351464

Stoll, M E; Vega, A J; Vaughan, R W

A double resonance multiple pulse nuclear magnetic resonance experiment is proposed and demonstrated which allows the use of heteronuclear dipolar interactions to determine geometrical, orientational, and motional information in polycrystalline solids. /sup 13/C--/sup 1/H double resonance experiments are performed in polycrystalline benzene and calcium formate to demonstrate the capabilities of the technique in its present form. (AIP)

• Research Organization: California Institute of Technology, Pasadena, California 91125
• OSTI ID: 7351464
• Journal Information: J. Chem. Phys.; (United States), Journal Name: J. Chem. Phys.; (United States) Vol. 65:10; ISSN JCPSA
• Country of Publication: United States
• Language: English

Related Subjects

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CHEMISTRY
400202* -- Isotope Effects
Isotope Exchange
& Isotope Separation
ALKALINE EARTH METAL COMPOUNDS
AROMATICS
BENZENE
CALCIUM COMPOUNDS
CARBON 13
CARBON ISOTOPES
CARBOXYLIC ACID SALTS
EVEN-ODD NUCLEI
FORMATES
HYDROCARBONS
ISOTOPE EFFECTS
ISOTOPES
LIGHT NUCLEI
MAGNETIC RESONANCE
NUCLEAR MAGNETIC RESONANCE
NUCLEI
ORGANIC COMPOUNDS
RESONANCE
STABLE ISOTOPES