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Indentation studies on Y[sub 2]O[sub 3]-stabilized ZrO[sub 2]; 2: Toughness determination from stable growth of indentation-induced cracks

Journal Article · · Journal of the American Ceramic Society; (United States)
;  [1]; ;  [2];  [3];  [4]
  1. Inst. fuer Reaktorwerkstoffe, Juelich (Germany)
  2. Univ. de Extremadura, Badajoz (Spain). Facultad de Ciencias
  3. Univ. de Sevilla (Spain). Dept. de Fisic Materia Condensada
  4. Case Western Reserve Univ., Cleveland, OH (United States). Dept. of Materials Science and Engineering

Stable indentation cracks were grown in four-point bend tests to study the fracture toughness of two Y[sub 2]O[sub 3]-stabilized ZrO[sub 2] ceramics containing 3 and 4 mol% Y[sub 2]O[sub 3]. By combining microscopic in situ stable crack growth observations at discrete stresses with crack profile measurements, the dependence of toughness on crack extension was determined from crack extension plots, which graphically separate the crack driving residual stress intensity and applied stress intensity factors. Both materials exhibit steeply rising R-curves, with a plateau toughness of 4.5 and 3.1 MPa[center dot]m[sup 1/2] for the 3- and 4-mol% materials, respectively. The magnitude of the plateau toughness reflects the fraction of tetragonal grain contributing to transformation toughening.

OSTI ID:
7303142
Journal Information:
Journal of the American Ceramic Society; (United States), Journal Name: Journal of the American Ceramic Society; (United States) Vol. 77:5; ISSN 0002-7820; ISSN JACTAW
Country of Publication:
United States
Language:
English