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Two pyrene derivatives of widespread environmental distribution: cyclopenta(cd)pyrene and acepyrene. [Carcinogenesis; soots; coal tar pitch]

Journal Article · · Environ. Sci. Technol.; (United States)
DOI:https://doi.org/10.1021/es60100a002· OSTI ID:7196866

An orange polycyclic aromatic hydrocarbon with reported tumorigenic properties, isolated from carbon black and other soots by several previous investigators, was identified as cyclopenta(cd)pyrene. This compound is the first known cycloalkenyl pyrene derivative. It was characterized by elemental analysis, proton magnetic resonance, mass spectroscopy and uv-vis spectroscopy. A benzene extract of the carbon black used for its isolation contained 60-fold more cyclopenta(cd)pyrene than benzo(a)pyrene. Hydrogenation of cyclopenta(cd)pyrene yielded acepyrene (3,4-dihydrocyclopenta(cd)pyrene). The latter hydrocarbon is present in relatively abundant concentrations in coal tar pitch. The mass spectrum, proton magnetic resonance spectrum, and quantitative uv spectrum of acepyrene are reported.

Research Organization:
Univ. of Nebraska Medical Center, Omaha
OSTI ID:
7196866
Journal Information:
Environ. Sci. Technol.; (United States), Journal Name: Environ. Sci. Technol.; (United States) Vol. 9:2; ISSN ESTHA
Country of Publication:
United States
Language:
English