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A radiocarbon tracer method for measuring tropospheric OH

Thesis/Dissertation ·
OSTI ID:7195993
A radiochemical method for measuring the ground-level ambient hydroxyl radical (OH) concentration was refined. The method uses {sup 14}CO as a tracer of the atmospheric OH-CO reaction in a UV transparent photochemical reactor. The OH concentration is inferred from the resulting {sup 14}CO{sub 2} activity, reaction time, tracer concentration, and CO-OH reaction rate constant. The causes of the highly variable measurements obtained with the method prior to 1985 were overcome with the development of an isotopic-dilution system for the purification of the {sup 14}CO{sub 2}, and a column packed with porous polymer beads for the removal of the interfering ambient {sup 222}Rn. In contrast to other methods, which are limited by atmospheric concentration fluctuations, precision of the Radiocarbon Tracer method is limited only by {sup 14}C counting uncertainty. Therefore, refinements of purification techniques could result in an OH detection limit of about 10{sup 4} radicals cm{sup {minus}3}. Forty-three experiments performed on five days in October 1987 revealed the first tropospheric OH variations ever reproduced. Calculations with a non-steady-state photochemical model with variable NO{sub x} concentrations agreed with clean air OH measurements performed near Colfax, WA and others.
Research Organization:
Washington State Univ., Pullman, WA (USA)
OSTI ID:
7195993
Country of Publication:
United States
Language:
English