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Acidity and catalytic activity of MeAPSO-34 (Me = Co, Mn, Cr), SAPO-34, and H-ZSM-5 molecular sieves in methanol dehydration

Journal Article · · Journal of Catalysis; (United States)
 [1];  [2]
  1. Boris Kidric Inst. of Chemistry, Ljubljana (Slovenia)
  2. Univ. of Ljubljana (Slovenia)

SAPO-34 and the isomorphously substituted MeAPSO-34 (Me = Co, Mn, Cr) molecular sieves have been synthesized. Temperature-programmed desorption (TPD) profiles and the reaction rates of methanol dehydration have been measured on these samples in comparison with H-ZSM-5. The acidity strength of samples has been determined qualitatively from the temperatures of dimethyl ether desorption peaks, and the following sequence has been obtained: H-ZSM-5 > MnAPSO-34 > CoAPSO-34 > CrAPSO-34 > SAPO-34. The following sequence of catalytic acitivty has been observed: H-ZSM-5 [much gt] SPAO-34 > CrAPSO-34 > CoAPSO-34 > MnAPSO-34. The selectivities for the formation of low olefines have been observed to decrease rapidly with time on stream for all catalysts in the SAPO-34 and MeAPSO-34 series as a consequence of coking. The highest selectivity to ethane production among these catalysts has been found for MnAPSO-34.

OSTI ID:
7189389
Journal Information:
Journal of Catalysis; (United States), Journal Name: Journal of Catalysis; (United States) Vol. 135:2; ISSN 0021-9517; ISSN JCTLA5
Country of Publication:
United States
Language:
English

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