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Title: Effect of extended solid solution of Hf on the microstructure of the laser clad Ni-Fe-Cr-Al-Hf alloys

Technical Report ·
OSTI ID:7161596

Alloys and coatings for alloys for improved high-temperature service life under aggressive atmospheres are of great contemporary interest. There is a general consensus that addition of reactive elements such as Hf will provide many beneficial effects for such alloys. The laser cladding technique was used to produce Ni-Fe-Cr-Al-Hf alloys with extended solid solution of Hf. A 10-kW CO/sub 2/ laser with mixed powder feed was used for laser cladding. Optical, scanning electron (SEM) and scanning transmission electron (STEM) microscopy were employed for microstructural evolution of alloys produced during laser-cladding processes. The electron probe microanalysis and the Auger electron spectroscopy were also used for microchemical analysis of different phases. Microstructural studies revealed a high degree of grain refinement, considerable increase in solubility of Hf in matrix, and Hf-rich precipitates and new metastable phases. This paper reports the microstructural development in this laser-clad Ni-Fe-Cr-Al-Hf alloy.

Research Organization:
Illinois Univ., Urbana (USA). Laser Aided Materials Processing Lab.
OSTI ID:
7161596
Report Number(s):
AD-A-191460/5/XAB
Resource Relation:
Other Information: Pub. in Acta Metallurgica, Vol. 35, No. 8, 1995-2003(1987)
Country of Publication:
United States
Language:
English