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High resolution NMR in randomly oriented solids with homonuclear dipolar broadening: Combined multiple pulse NMR and magic angle spinning

Journal Article · · J. Chem. Phys.; (United States)
DOI:https://doi.org/10.1063/1.433638· OSTI ID:7135458
; ; ;
The first combined multiple pulse-magic angle experiment is reported in which both homonuclear dipole interactions and chemical shift anisotropies are removed to resolve chemically shifted fluorines. The sample selected was KEL-F.(AIP) (AIP)
Research Organization:
Ames Laboratory-ERDA and Department of Chemistry, Iowa State University, Ames, Iowa 50011
OSTI ID:
7135458
Journal Information:
J. Chem. Phys.; (United States), Journal Name: J. Chem. Phys.; (United States) Vol. 66:1; ISSN JCPSA
Country of Publication:
United States
Language:
English

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Related Subjects

36 MATERIALS SCIENCE
360404* -- Materials-- Polymers & Plastics-- Physical Properties-- (-1987)
37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CHEMISTRY
400301 -- Organic Chemistry-- Chemical & Physicochemical Properties-- (-1987)
ACCURACY
CHEMICAL SHIFT
GYROMAGNETIC RATIO
KEL-F
MAGNETIC RESONANCE
NUCLEAR MAGNETIC RESONANCE
ORGANIC CHLORINE COMPOUNDS
ORGANIC COMPOUNDS
ORGANIC FLUORINE COMPOUNDS
ORGANIC HALOGEN COMPOUNDS
ORGANIC POLYMERS
POLYETHYLENES
POLYMERS
POLYOLEFINS
RESONANCE