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U.S. Department of Energy
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Interface engineering in oxide fiber/oxide matrix composites. Annual report, 1 March 1993-28 February 1994

Technical Report ·
OSTI ID:7114647
The authors have shown in earlier work that significant improvements in the mechanical properties of the alumina + 15 w/o zirconia (PRD-166) fiber/borosilicate glass matrix and mullite (Nextel 480 and 550) fiber/mullite matrix composites could be achieved using an interface engineering approach. This approach involves a control of the microstructure, roughness of the interface, and the thermal expansion mismatch between the fiber and matrix in order to improve the strength and fracture toughness of the composite. They have made a qualitative comparison of the elemental distribution in the PRD-166/glass (N51A) composites, with and without and SnO2 coating, on fibers using secondary ion mass spectrometry (SIMS). The results confirmed that tin dioxide serves as an effective barrier between this fiber and the silica-based glass. The tensile strength and toughness of the interface between SnO2 and flat alumina substrate were obtained by a laser spallation technique.
Research Organization:
New Mexico Inst. of Mining and Technology, Socorro, NM (United States). Dept. of Metallurgical and Materials Engineering
OSTI ID:
7114647
Report Number(s):
AD-A-277672/2/XAB; CNN: N00014-89-J-1459
Country of Publication:
United States
Language:
English