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Methane oxidation over Pt on. gamma. -alumina: Kinetics and structure sensitivity

Journal Article · · Langmuir; (USA)
DOI:https://doi.org/10.1021/la00090a018· OSTI ID:7052880
 [1]
  1. Ford Motor Co., Dearborn, MI (USA)

A recirculation batch reactor and a mass spectrometer were used to measure methane oxidation rates, free of mass-transfer limitations, over Pt. Samples included platinum on {gamma}-alumina in the range from 0.03 to 30 wt% and Pt black. The reaction is described by first-order kinetics with respect to methane and is independent of oxygen pressure under the experimental conditions chosen. A maximum in turnover frequency and a decrease in apparent activation energy with increasing Pt concentration are found. Calculations of a reaction site density, based on theoretical and empirical kinetics, are inconsistent with an Eley-Rideal reaction mechanism. The reaction is possibly rate controlled by the dissociation of methane.

OSTI ID:
7052880
Journal Information:
Langmuir; (USA), Journal Name: Langmuir; (USA) Vol. 5:6; ISSN LANGD; ISSN 0743-7463
Country of Publication:
United States
Language:
English