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Radiation effects in amorphous Fe/sub x/Ni/sub 80-x/P/sub 14/B/sub 6/

Technical Report ·
DOI:https://doi.org/10.2172/7052386· OSTI ID:7052386

Changes in the Curie temperature and magnetic saturation of the amorphous ferromagnetic series Fe/sub x/Ni/sub 80-x/P/sub 14/B/sub 6/ for 20 less than or equal to x less than or equal to 34 induced by proton bombardment have been studied, and correlated with small angle x-ray scattering measurements performed for x = 20 at Oak Ridge National Laboratory. Both the Curie temperature and the low temperature saturation magnetization increase with proton fluence up to 10/sup 16/ cm/sup -2/ but are constant for higher fluences. Protons of energy 2.25 MeV (range much greater than the sample thickness) are more effective at producing changes than protons of energy 0.25 MeV (range much less than sample thickness). Thus, hydrogen implantation is eliminated as the principal source of the observed changes. In addition, careful attention to sample temperature during irradiation excludes thermal annealing as the origin of the effect. Proton bombardment at the same fluences produces scattering centers that are observed by small angle x-ray scattering. The concentration of scattering centers increases with proton fluence up to 10/sup 16/ cm/sup -2/, but remains constant thereafter. The size of the centers remains constant at about 16 to 30 A. Possible structural changes to account for these observations are incipient recrystallization, void formation, and phosphorous segregation.

Research Organization:
Delaware Univ., Newark, DE (USA)
Sponsoring Organization:
USDOE
DOE Contract Number:
AC02-80ER10571
OSTI ID:
7052386
Report Number(s):
DOE/ER/10571-2
Country of Publication:
United States
Language:
English