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In-situ sulfur dioxide capture by flame-injected sorbents

Thesis/Dissertation ·
OSTI ID:7016134

The author has burned 52 coal-volatiles-like (doped with sulfur dioxide) float flames that simulate well the early stages of coal combustion, as well as provided good times/temperature resolution. The experimental and theoretical research program of SO/sub 2/ capture lead to the following findings. (1) Significant (20-50%) SO/sub 2/ capture occurs rapidly (2.5 milliseconds) in the early zones of coal volatiles-like flames. (2) Increasing residence time did not necessarily increase the SO/sub 2/ capture efficiency. (3) For non-precalcined sorbents, SO/sub 2/ capture was proportional to (Ca/5)/sup x/, x = 0.21-0.43. For the partly-precalcined sorbents, capture was proportional to (Ca/S)/sup y/, y = 0.60-0.77. (4) SO/sub 2/ capture doubled when N/sub 2/ replaced CO/sub 2/ as the inert component of the oxidant. (5) At lower temperatures (1279-1383 K) in CO/sub 2/-containing flames, no significant effect of equivalence ratio on SO/sub 2/ capture was observed for all sorbents. In N/sub 2/-containing flames (1369-1417 K), fuel-lean (0 = 0.8) conditions favored SO/sub 2/ capture over fuel-rich ( 0 = 1.2) conditions for all sorbents. SO/sub 2/ capture for the stoichiometric condition was randomly above, between, or below that for either fuel-lean or fuel-rich conditions. (5) For all equivalence ratios, one sorbent exhibited the most efficient capture of SO/sub 2/ because of its having the highest porosity, the smallest mean-volume diameter, some pre-calcination, and considerably high surface area. (7) SO/sub 2/ capture data from experiments could be predicted quite successfully using a modified pore tree model and by adjusting the global rate coefficient and global reaction exponent of SO/sub 2/ concentration.

Research Organization:
Pennsylvania State Univ., University Park (USA)
OSTI ID:
7016134
Country of Publication:
United States
Language:
English