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Calibrating a vacuum ionization gauge for hydrogen using a frit-type plugging meter

Journal Article · · Nuclear Technology; (USA)
OSTI ID:7013755
 [1]
  1. Argonne National Lab., Idaho Falls, ID (USA)
The hydrogen meter leak detectors at the Experimental Breeder Reactor II (EBR-II) are periodically checked with a vacuum ionization gauge to see if the leak detectors are calibrated. The gauge, which measures equilibrium pressure, requires an equation to convert the gauge pressure to the hydrogen concentration in sodium. The original equation is derived from Sievert's law with adjustments for gauge sensitivity to hydrogen and thermal transpiration effects. EBR-II experience has shown that the Sievert's law equation has not been reliable in accurately determining the hydrogen concentration in sodium. It is also difficult to determine the hydrogen gauge sensitivity, which can change with time. This paper reports the development of a new equation over a hydrogen range of 0.063 to 0.230 ppm, by using a frit-type plugging meter to determine the hydrogen concentration when an equilibrium pressure measurement is done. With sodium hydride as the predominant impurity, the impurity saturation temperature (plugging temperature) measured with the plugging meter can be used to calculate the hydrogen concentration.
OSTI ID:
7013755
Journal Information:
Nuclear Technology; (USA), Journal Name: Nuclear Technology; (USA) Vol. 88:3; ISSN NUTYB; ISSN 0029-5450
Country of Publication:
United States
Language:
English