A new phase in the Sr-Pb-Cu oxide system: The crystal structure of Sr sub 5-x Pb sub 3+x Cu sub y O sub 12-. delta
Journal Article
·
· Journal of Solid State Chemistry; (USA)
- Univ. of Texas, Austin (USA)
A single crystal with compositions Sr{sub 4.79}Pb{sub 3.21}Cu{sub 0.66}O{sub 11.12} was grown from a reaction mixture of nominal composition 2 Pb: 1 Sr: 1 Cu that was fired at 860{degree}C in air. M{sub r} = 1304.6, hexagonal, P{bar 6}2m, a = 10.072(3) {angstrom}, c = 3.542(3) {angstrom}, V = 311.2(4) {angstrom}{sup 3}, Z = 1, Dx = 6.96 g cm{sup {minus}3}, {lambda} = 0.71069 {angstrom}, {mu} = 645 cm{sup {minus}1}, F(000) = 553.34, room temperature, R = 0.040 for 323 unique reflections > 5{sigma} (F{sub 0}).
- OSTI ID:
- 6926384
- Journal Information:
- Journal of Solid State Chemistry; (USA), Journal Name: Journal of Solid State Chemistry; (USA) Vol. 85:1; ISSN 0022-4596; ISSN JSSCB
- Country of Publication:
- United States
- Language:
- English
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Related Subjects
36 MATERIALS SCIENCE
360201* -- Ceramics
Cermets
& Refractories-- Preparation & Fabrication
360202 -- Ceramics
Cermets
& Refractories-- Structure & Phase Studies
ALKALINE EARTH METAL COMPOUNDS
CHALCOGENIDES
COMPOSITE MATERIALS
COPPER COMPOUNDS
COPPER OXIDES
CRYSTAL STRUCTURE
DATA
DATA ANALYSIS
EXPERIMENTAL DATA
INFORMATION
LEAD COMPOUNDS
MATERIALS
MEASURING INSTRUMENTS
MEASURING METHODS
NUMERICAL DATA
OXIDES
OXYGEN COMPOUNDS
PHASE STUDIES
STRONTIUM COMPOUNDS
SUPERCONDUCTING COMPOSITES
SYNTHESIS
TRANSITION ELEMENT COMPOUNDS
360201* -- Ceramics
Cermets
& Refractories-- Preparation & Fabrication
360202 -- Ceramics
Cermets
& Refractories-- Structure & Phase Studies
ALKALINE EARTH METAL COMPOUNDS
CHALCOGENIDES
COMPOSITE MATERIALS
COPPER COMPOUNDS
COPPER OXIDES
CRYSTAL STRUCTURE
DATA
DATA ANALYSIS
EXPERIMENTAL DATA
INFORMATION
LEAD COMPOUNDS
MATERIALS
MEASURING INSTRUMENTS
MEASURING METHODS
NUMERICAL DATA
OXIDES
OXYGEN COMPOUNDS
PHASE STUDIES
STRONTIUM COMPOUNDS
SUPERCONDUCTING COMPOSITES
SYNTHESIS
TRANSITION ELEMENT COMPOUNDS