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Reactivity and acidity of Li in LiAlO[sub 2] phases

Journal Article · · Inorganic Chemistry; (United States)
DOI:https://doi.org/10.1021/ic00053a001· OSTI ID:6837438
 [1]
  1. Cornell Univ., Ithaca, NY (United States)

Nuclear physicists were interested in the [gamma]-modification of LiAlO[sub 2]. Because of its good performance under high neutron and electron radiation, the phase appears to be a promising lithium ceramic suitable as an in situ trituim-breeding material in future fusion reactors. With the help of semiempirical electronic structure calculations, the authors seek to understand why solid [alpha]-LiAlO[sub 2] exchanges Li[sup +] with H[sup +] while in contact with molten benzoic acid but [gamma]-LiAlO[sub 2] does not. After critically examining the structural data for LiAlO[sub 2] modifications, they calculate the binding and both the static and dynamic reactivity and the static and dynamic acidity of [alpha]- and [gamma]-LiAlO[sub 2], with a special interpretative emphasis on the Li ion. The reason for Li being solely extractable in [alpha]-LiAlO[sub 2] is found to arise from (1) a difference in Li electrophilicity between [alpha]- and [gamma]-phase (frontier band argument), (2) a significantly smaller energy for Li binding to its neighboring atoms in [alpha]-compared to [gamma]-phase (thermodynamic argument), and (3) a dramatic difference in energetic behavior upon dislocating a Li atom from its equilibrium position in [alpha]- and [gamma]-phase (kinetic argument). Additionally, the authors show how the movement of a local atomic carrier of reactivity and acidity within a nonequilibrium structure can be easily observed by use of computation. 64 refs., 12 figs., 3 tabs.

OSTI ID:
6837438
Journal Information:
Inorganic Chemistry; (United States), Journal Name: Inorganic Chemistry; (United States) Vol. 32:1; ISSN 0020-1669; ISSN INOCAJ
Country of Publication:
United States
Language:
English