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Title: CNG acid-gas-removal process. Technical progress report 4 for the period 1 August 1981-31 October 1981

Technical Report ·
OSTI ID:6830099

Four tasks were active: design and construction of a bench-scale triple-point crystallizer; equilibrium data acquisition, crystallizer separation factors for several sulfur-containing molecules and trace contaminants, and slurry pumping. A new design for the CNG crystallizer has been completed. A control scheme was devised for the new design. Equipment sizing, selection, and procurement is in progress. Equilibrium data acquisition has been completed. Five component vapor-liquid equilibrium data for gas mixtures representative of BCR Bi-Gas and Exxon catalytic gasifier crude gases were measured. The experimental data agree very well with the equilibrium data estimated by computer calculations. Separation factors were determined for the binary systems carbon dioxide/hydrogen sulfide, carbon dioxide/carbonyl sulfide, carbon dioxide/ethane, carbon dioxide/ethylene, and carbon dioxide/methyl mercaptan. For each system, sharp separation was observed in one stage of crystallization. In the slurry pumping project the height of liquid leg between the free flashing surface and the pump centerline is being varied to determine the minimum suction head needed for pumping slurry. The pump in current use is a MICROPUMP gear pump.

Research Organization:
Helipump Corp., Cleveland, OH (USA)
DOE Contract Number:
AC21-80MC14399
OSTI ID:
6830099
Report Number(s):
DOE/MC/14399-T3; ON: DE82022218
Country of Publication:
United States
Language:
English