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Nickel, copper and vanadyl porphyrins from Moroccan oil shales. Composition, novel structures, biological precursors

Conference · · American Chemical Society, Division of Petroleum Chemistry, Preprints; (USA)
OSTI ID:6820530

An exhaustive structural investigation of the nickel and vanadyl-porphyrin fractions from two Moroccan oil shales, Timahdit and Oulad Abdoun, was carried out. More than 20 structures, half of them showing a novel carbon skeleton, were unambiguously assigned by combined spectroscopic (FT NMR + nOe) and synthetic (total or partial synthesis) methods. In addition to the classical series, two groups of structures are of particular interest: (a) the tetrahydrobenzoporphyrins which might derive from a still unknown family of natural chlorophylls; (b) the 17-nor-DPEPs which are likely fossils of the algal chlorophyll c. The last series is complementary to the known 15,17-ethanoporphyrins, specific markers for chlorophyll c and the distribution of both series in various oil shales will be discussed. The composition of a minor copper-porphyrin fraction and preliminary indications concerning the free bases from Oulad Abdoun oil shale will also be presented.

OSTI ID:
6820530
Report Number(s):
CONF-8904127--
Journal Information:
American Chemical Society, Division of Petroleum Chemistry, Preprints; (USA), Journal Name: American Chemical Society, Division of Petroleum Chemistry, Preprints; (USA) Vol. 34:1; ISSN 0569-3799; ISSN ACPCA
Country of Publication:
United States
Language:
English