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Title: EDS coal liquefaction process development: Phase IIIA. Monthly technical progress report, June 1--June 30, 1977

Technical Report ·
DOI:https://doi.org/10.2172/6812836· OSTI ID:6812836

Highlights from this report are summarized as follows. With the 50 pound-per-day Recycle Coal Liquefaction Unit (RCLU), the effect of recycling coker liquids derived from Illinois No. 6 coal on liquefaction was investigated. Operations with Wyoming coal were conducted using a recycle solvent heavier than that typically used. Following the completion of the sixteen-day Wyoming coal run on the one ton-per-day Coal Liquefaction Pilot Plant (CLPP) an inspection revealed that high erosion rates had occurred in the vacuum flash feed zone. A preliminary liquefaction model for Wyodak coal has been developed which correlates 1000/sup 0/F+ bottoms yield as a function of temperature and residence time. Raw 400-1000/sup 0/F EDS coal liquid burned clean in a 50 horsepower pilot scale industrial boiler. Smoke and particulate emission levels for the coal liquid were significantly lower than values obtained with a reference petroleum fuel oil. A preliminary study indicates the optimum feed ash level for Illinois coal is probably not significantly different than that used in the Illinois Study Design. A preliminary evaluation of air-blown, moving-bed gasification (MBG) has been completed. The low Btu gas (LBG) produced by the MBG process is more expensive to make than LBG from coal FLEXICOKING, although both options produce fuel of significantly lower cost than high Btu gas or liquids. More than 90% of the phenolic compounds were removed from CLPP waste water by solvent extraction.

Research Organization:
Exxon Research and Engineering Co., Baytown, Tex. (USA). Baytown Research and Development Div.
DOE Contract Number:
EX-76-C-01-2353
OSTI ID:
6812836
Report Number(s):
FE-2353-18
Country of Publication:
United States
Language:
English