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Title: Processing aqueous effluent liquors from degasification or gasification of coal

Patent ·
OSTI ID:6799165

The aqueous effluent liquors from gasification or degasification of coal are extracted with a water-insoluble solvent and the extract is processed to recover the solvent. The aqueous residue is treated to remove nh3 in a driving-off column. The invention adds the steps of (A) removing part of the overhead product of the driving-off column as uncondensed vapors; (B) transferring the vapors from (A) to a scrubbing column, in steps condensing water, small amounts of ammonia and all acid gases in the upper part of said scrubbing column, and withdrawing pure ammonia overhead; (C) withdrawing the condensate which contains all acid gases from the upper portion of the scrubbing column, transferring the condensate to a separate reboiler, and heating the transferred condensate in said reboiler; (D) feeding cold water at a low rate to the top of the scrubbing column; (E) withdrawing the sump product of the scrubbing column, transferring it into a pressurized de-acidification column, and withdrawing therefrom overhead under pressure the acid gases h2s and co2; and (F) recycling to the stripping column the sump product of the pressurized de-acidification column consisting of a solution high in ammonia content.

Assignee:
Metallgesellschaft Ag (Germany, Federal Republic Of)
Patent Number(s):
US 4240808
OSTI ID:
6799165
Resource Relation:
Patent Priority Date: Priority date 3 Oct 1977, German, Federal Republic of (F.R. Germany)
Country of Publication:
United States
Language:
English