Existing technology transfer report: analytical capabilities. Appendix B. Volume 3
The overall objective of the on-going analytical efforts was to develop in-house expertise and analytical capability for the analysis of coal and coal-derived products in support of SRC-I process technology. The approach taken and work accomplished involved: identification of test methods and associated equipment; review and implementation of analytical facility plan; evaluation of existing instrumentation; evaluation and purchase of new instruments; training of laboratory personnel; validation or development of analytical methods; development of standard product work-up methods and development of analytical protocol for detailed characterization of SRC-I solid and liquid products. This volume contains Appendix B with the following attachments: solvent separation procedure A; Wilsonville solvent separation procedure, distillation separation procedure; solvent separation modified Wilsonville Procedure W; statistical comparison of 3 solvent separation procedures; methods development for column chromatography, and application of gas chromatography to characterization of a hydrogen donor solvent; and high performance liquid chromatographic procedure.
- Research Organization:
- Air Products and Chemicals, Inc., Allentown, PA (USA)
- DOE Contract Number:
- AC05-78OR03054
- OSTI ID:
- 6615333
- Report Number(s):
- DOE/OR/03054-116-Vol.3; ON: DE85001636
- Country of Publication:
- United States
- Language:
- English
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Related Subjects
010405 -- Coal
Lignite
& Peat-- Hydrogenation & Liquefaction
010600* -- Coal
Lignite
& Peat-- Properties & Composition
CARBONACEOUS MATERIALS
CHEMICAL ANALYSIS
CHROMATOGRAPHY
COAL
COAL LIQUIDS
DISTILLATION
ENERGY SOURCES
EXTRACTION
FLUIDS
FOSSIL FUELS
FUELS
GAS CHROMATOGRAPHY
LIQUID COLUMN CHROMATOGRAPHY
LIQUIDS
MATERIALS
MEASURING METHODS
SEPARATION PROCESSES
SOLVENT EXTRACTION
SRC PROCESS