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An investigation of adducts of arsonic acids with amines by nuclear quadrupole resonance of /sup 75/As nuclei

Journal Article · · Bull. Acad. Sci. USSR, Div. Chem. Sci. (Engl. Transl.); (United States)
OSTI ID:6593059
The /sup 75/As nuclear quadrupole resonance (NQR) spectra of the adducts of arsonic acids with amines of the general formula RAs(O)(OH)/sub 2/NR'/sub 3/ were studied. The adducts were synthesized by direct mixing of alcoholic solutions of arsonic acids with amines. A wide range of derivatives of arsonic acids with different pK/sub a/ values and aliphatic primary and secondary amines with different basicities were investigated by physicochemical methods. /sup 75/As NQR spectra of adducts of arsonic acids and amines in a crystalline phase were measured at 77/sup 0/K on an IS-3 NQR pulse spectrometer. Complete proton transfer from the molecule of the acid to the amine in adducts of arsonic acids with amines was postulated from this investigation.
Research Organization:
Academy of Sciences of the USSR, Kazan
OSTI ID:
6593059
Journal Information:
Bull. Acad. Sci. USSR, Div. Chem. Sci. (Engl. Transl.); (United States), Journal Name: Bull. Acad. Sci. USSR, Div. Chem. Sci. (Engl. Transl.); (United States) Vol. 30:9; ISSN BACCA
Country of Publication:
United States
Language:
English