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Predicting and modeling the low-voltage cathodoluminescent efficiency of oxide phosphors

Journal Article · · Journal of the Electrochemical Society
DOI:https://doi.org/10.1149/1.1838781· OSTI ID:659121
;  [1];  [2]
  1. Univ. of California, San Diego, La Jolla, CA (United States)
  2. Sandia National Labs., Albuquerque, NM (United States)

A novel ceramic synthesis technique, combustion synthesis, was used to produce submicron-sized Y{sub 2}O{sub 3}:Eu{sup 3+} phosphors. This technique exploits the exothermic redox reaction of yttrium and europium nitrates (oxidizers) with urea (CH{sub 4}N{sub 2}O) fuel (reducing agent). Resulting powders were luminescent in the as-synthesized state. However, their luminous intensity increased with increasing postreaction annealing treatments (1,000--1,600 C for 2 h). The low-voltage (200--1,000 V) cathodoluminescence efficiency of Y{sub 2}O{sub 3}:Eu{sup 3+} was found to increase with increasing crystallite size, independent of the particle size. A model of low-voltage cathodoluminescence that includes the effects of the crystallite size, the probability of radiative recombination, and the effect of surface-bound electrons was developed to predict phosphor efficiency at low voltages. The efficiencies predicted by the model are in very good agreement with experimental results.

Sponsoring Organization:
USDOE
OSTI ID:
659121
Journal Information:
Journal of the Electrochemical Society, Journal Name: Journal of the Electrochemical Society Journal Issue: 9 Vol. 145; ISSN JESOAN; ISSN 0013-4651
Country of Publication:
United States
Language:
English