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Production of the ammonium salt of 3,5-dinitro-1,2,4-triazole by solvent extraction

Patent ·
OSTI ID:6586650
;

The ammonium salt of 3,5-dinitro-1,2,4-triazole has utility as a chemical explosive. In accordance with the present invention, it may readily be produced by solvent extraction using high molecular weight, water-insoluble amines followed by amination with anhydrous ammonia gas. The aqueous reaction mixture produced in the synthesis of the parent compound, 3,5-dinitro-1,2,4triazole, is quite suitable--and indeed is preferred--for use as the feed material in the process of the invention.

Assignee:
Department of Energy
Patent Number(s):
US 4236014
OSTI ID:
6586650
Country of Publication:
United States
Language:
English

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Related Subjects

45 MILITARY TECHNOLOGY, WEAPONRY, AND NATIONAL DEFENSE
450100* -- Military Technology
Weaponry
& National Defense-- Chemical Explosions & Explosives
AMMONIUM COMPOUNDS
AZOLES
CHEMICAL EXPLOSIVES
CHEMICAL PREPARATION
EXPLOSIVES
EXTRACTION
HETEROCYCLIC COMPOUNDS
ORGANIC COMPOUNDS
ORGANIC NITROGEN COMPOUNDS
SEPARATION PROCESSES
SOLVENT EXTRACTION
SYNTHESIS
TRIAZOLES