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Thermodynamics of sulfur chemisorption on metals. II. Alumina-supported ruthenium

Journal Article · · J. Chem. Phys.; (United States)
DOI:https://doi.org/10.1063/1.440905· OSTI ID:6582361

Isosteric heats of chemisorption of sulfur on alumina-supported ruthenium have been determined by measuring the equilibrium ratio of H/sub 2/S/H/sub 2/ in contact with the solid in a closed gas-recirculation system. At low coverage the heat of chemisorption with respect to 1/2 S/sub 2/(g) was found to be -215 +- 15 kJ mol/sup -1/. With increasing coverage it decreased to -174 +- 10 kJ mol/sup -1/, a value comparable to the heat of formation of bulk ruthenium sulfide. For equal coverage with sulfur, the thermodynamic chemical potential of alumina-supported ruthenium exceeds that of alumina-supported nickel by approximately one order of magnitude. The binding strength of adsorbed sulfur is 432 +- 15 kJ mol/sup -1/ for Ru and 464 +- 15 kJ mol/sup -1/ for Ni.

Research Organization:
Solid State Catalysis Laboratory, SRI International, Menlo Park, California 94025
OSTI ID:
6582361
Journal Information:
J. Chem. Phys.; (United States), Journal Name: J. Chem. Phys.; (United States) Vol. 74:10; ISSN JCPSA
Country of Publication:
United States
Language:
English