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Micro-magnetic susceptometer for the actinides

Conference ·
OSTI ID:6581776
A D.C. magnetic susceptometer incorporating a SQUID as a magnetic flux sensor has been constructed with sensitivity to measure the magnetic susceptibility of submicrogram actinide samples as a function of temperature. For a two microgram actinide sample the minimum measurable dimensionless susceptibility is approximately 10/sup -7/ CGS in a 2000 gauss field. The sensitivity has been determined in a series of calibration experiments using samples of lead spheres at 4.2/sup 0/K. Pick-up coils insensitive to changes in spatially uniform fields and fields with a constant first derivative were used to reduce noise. The field was trapped in a niobium cylinder to produce a uniform stable applied field. The flux produced by the sample in the pick-up coils is proportional to the magnetic susceptivility of the sample and is a function of the sample position.
Research Organization:
Tennessee Univ., Knoxville (USA); Oak Ridge National Lab., TN (USA)
DOE Contract Number:
W-7405-ENG-26
OSTI ID:
6581776
Report Number(s):
CONF-780823-6
Country of Publication:
United States
Language:
English