Design and thermal stress analysis of high-power x-ray monochromators cooled with liquid nitrogen

Journal Article · Wed Feb 01 04:00:00 EST 1995 · Review of Scientific Instruments; (United States)

DOI:https://doi.org/10.1063/1.1145705· OSTI ID:6580326

Rogers, C S; Assoufid, L ^[1]

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1. Experimental Facilities Division, Advanced Photon Source, Argonne National Laboratory, Argonne, Illinois 60439-4814 (United States)

Cryogenically cooled, single-crystal silicon, x-ray monochromators offer much better thermal performance than room-temperature silicon monochromators. The improved performance can be quantified by a figure-of-merit equal to the ratio of the thermal conductivity to the coefficient of thermal expansion. This ratio increases by about a factor of 50 as the temperature is decreased from 300 to 100 K. An extensive thermal and structural finite element analysis is presented for an inclined, liquid-nitrogen-cooled, Si monochromator crystal diffracting 4.2 keV photons from the [111] planes using undulator A at the Advanced Photon Source. The angular size of the beam accepted on the crystal was chosen to be 50 [mu]rad vertically and 120 [mu]rad horizontally. The deflection parameter, [ital K], was 2.17 for all cases. The peak power density at normal incidence to the beam was calculated to be 139 W/mm[sup 2], and the total power was 750 W at a distance of 30 m from the source for a positron current of 100 mA. The crystal was oriented in the inclined geometry with an inclination angle of 85[degree] for all cases. The performance of the crystal was investigated for beam currents of 100, 200, and 300 mA. The calculated peak slopes of the diffraction plane over the extent of the beam footprint were [minus]1.17, [minus]2.35, and 0.33 [mu]rad, and the peak temperatures were 88.2, 102.6, and 121.4 K, respectively. The variation in the Bragg angle due to change in [ital d] spacing across the beam footprint was less than 1 [mu]rad for all cases. These results indicate that a properly designed, cryogenically cooled, inclined silicon monochromator can deliver the full brilliance of undulator A at even the highest machine currents.

• Research Organization: Argonne National Laboratory (ANL), Argonne, IL
• DOE Contract Number: W-31109-ENG-38
• OSTI ID: 6580326
• Journal Information: Review of Scientific Instruments; (United States), Journal Name: Review of Scientific Instruments; (United States) Vol. 66:2; ISSN 0034-6748; ISSN RSINAK
• Country of Publication: United States
• Language: English

Related Subjects

43 PARTICLE ACCELERATORS
430303* -- Particle Accelerators-- Experimental Facilities & Equipment
ADVANCED PHOTON SOURCE
COOLING SYSTEMS
DESIGN
ELECTROMAGNETIC RADIATION
ELEMENTS
ENERGY SYSTEMS
EXPANSION
IONIZING RADIATIONS
MONOCHROMATORS
NITROGEN
NONMETALS
PHYSICAL PROPERTIES
RADIATION SOURCES
RADIATIONS
SEMIMETALS
SILICON
STRESSES
SYNCHROTRON RADIATION SOURCES
TEMPERATURE RANGE
TEMPERATURE RANGE 0065-0273 K
TEMPERATURE RANGE 0273-0400 K
THERMAL CONDUCTIVITY
THERMAL EXPANSION
THERMAL STRESSES
THERMODYNAMIC PROPERTIES
X RADIATION