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Ion beam studies of the reactions of atomic cobalt ions with alkanes: determination of metal-hydrogen and metal-carbon bond energies and an examination of the mechanism by which transition metals cleave carbon-carbon bonds

Journal Article · · J. Am. Chem. Soc.; (United States)
DOI:https://doi.org/10.1021/ja00394a010· OSTI ID:6572981

An ion beam apparatus is employed to study the reactions of singly charged cobalt positive ions with hydrogen and 17 alkanes. Reaction cross sections and product distributions as a function of kinetic energy are determined. Exothermic carbon-carbon bond cleavage reactions are observed for all alkanes but methane and ethane. A mechanism involving oxidative addition of C-C and C-H bonds to cobalt as a first step is demonstrated to account for all major reactions at all energies. Interpretation of several endothermic processes allows the extraction of thermochemical data. The bond dissociation energies obtained are D/sup 0/(Co/sup +/-H) = 52 +- 4 kcal/mol, D/sup 0/(Co-H) = 39 +- 6 kcal/mol, D/sup 0/(Co/sup +/-CH/sub 3/) = 61 +- 4 kcal/mol, and D/sup 0/(Co-CH/sub 3/) = 41 +- 10 kcal/mol.

Research Organization:
California Inst. of Tech., Pasadena
OSTI ID:
6572981
Journal Information:
J. Am. Chem. Soc.; (United States), Journal Name: J. Am. Chem. Soc.; (United States) Vol. 103:4; ISSN JACSA
Country of Publication:
United States
Language:
English