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Title: Spray forming lead strip. Final report

Technical Report ·
DOI:https://doi.org/10.2172/656791· OSTI ID:656791

A cooperative research project was conducted between the Idaho National Engineering Laboratory (INEL) and Johnson Controls, Inc. (JCI) to adapt the INEL spray forming process to produce near-net-shape lead alloy strip. The emphasis of the work was to spray form lead strip samples at INEL, using a variety of spray conditions, for characterization at JCI. An existing glove box apparatus was modified at INEL to spray form lead. The main spray forming components were housed inside the glove box. They included a spray nozzle, tundish (crucible), substrate assembly, gas heater and furnaces to heat the nozzle and tundish. To spray form metal strip, liquid metal was pressure-fed at a controlled rate through a series of circular orifices that span the width of the nozzle. There the metal contacted high velocity, high temperature inert gas (nitrogen) which atomized the molten material into fine droplets, entrained the droplets in a directed flow, and deposited them onto glass plates that were swept through the spray plume to form strip samples. In-flight convection cooling of the droplets followed by conduction and convection cooling at the substrate resulted in rapid solidification of the deposit. During operation, the inside of the glove box was purged with an inert gas to limit the effects of in-flight oxidation of the particles and spray-formed strips, as well as to protect personnel from exposure to airborne lead particulate. Remote controls were used to start/stop the spray and control the speed and position of the substrate. In addition, substrate samples were loaded into the substrate translator manually using the gloved side ports of the box. In this way, the glove box remained closed during a series of spray trials, and was opened only when loading the crucible with a lead charge or when removing lead strip samples for shipment to JCI.

Research Organization:
Lockheed Idaho Technologies Co., Idaho National Engineering and Environmental Lab., Idaho Falls, ID (United States)
Sponsoring Organization:
USDOE Office of Environmental Restoration and Waste Management, Washington, DC (United States)
DOE Contract Number:
AC07-94ID13223
OSTI ID:
656791
Report Number(s):
INEEL-97054490; ON: DE97054490; CRN: C/INEEL--95-CR-01; TRN: AHC29817%%350
Resource Relation:
Other Information: PBD: 10 Apr 1996
Country of Publication:
United States
Language:
English

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