Synthesis of 6-Methyl-9-n-propyldibenzothiophene-4-ol
The material presented here has been described to some extent in Status Reports 12, 13, and 14 and covers the progress toward the synthesis of the modified target molecules 9-isopropyl-4-methoxy-6-methyldibenzothiophene (13) and 9-isopropyl-6-methyldibenzothiophene-4-ol (14). It is divided into three parts: (a) Dehydrogenation experiments On tetrahydrodibenzothiophene 12. (b) methoxyl methyl cleavage of 13 to 14 using boron tribromide. (c) isolation and purification of methoxydibenzothiophene 13.
- Research Organization:
- Oklahoma State Univ., Stillwater, OK (United States)
- Sponsoring Organization:
- DOE; USDOE, Washington, DC (United States)
- DOE Contract Number:
- AC22-90PC90035
- OSTI ID:
- 6567223
- Report Number(s):
- DOE/PC/90035-T5; ON: DE93015776
- Country of Publication:
- United States
- Language:
- English
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