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An electron diffraction study of Bi sub 2 Sr sub 2 (Gd sub x Ca sub 1 minus x ) sub 0. 8 Cu sub 2 O sub 8+. delta

Journal Article · · Journal of Materials Research; (USA)
; ; ;  [1]
  1. Texas Center for Superconductivity, University of Houston, Houston, TX (USA)

The compound Bi{sub 2}Sr{sub 2}(Gd{sub {ital x}}Ca{sub 1{minus}{ital x}}){sub 0.8}Cu{sub 2}O{sub 8+{delta}} is examined by electron diffraction for several values of {ital x}. The incommensurate modulation which has been reported for {ital x}=0 persists for all values of {ital x} with the wave vector increasing as {ital x} increases. A secondary modulation with a wave vector equal to one half that of the primary is observed for {ital x}{ge}0.85. This modulation manifests itself through satellite reflections that are highly streaked normal to the (001) planes and that flank certain select positions in reciprocal space. The appearance of this secondary modulation is accompanied by a change in the average crystal structure from {ital B}-centered to {ital F}-centered orthorhombic.

OSTI ID:
6550309
Journal Information:
Journal of Materials Research; (USA), Journal Name: Journal of Materials Research; (USA) Vol. 5:8; ISSN JMREE; ISSN 0884-2914
Country of Publication:
United States
Language:
English