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U.S. Department of Energy
Office of Scientific and Technical Information

Alloy evaluation for fossil fuel process plants: liquefaction

Conference ·
OSTI ID:6528579
Since petroleum refinery pressure vessels are constructed of 2-1/4 Cr-1Mo steel (A387--74A-Gr.22-Cl.2) with a stainless steel weld overlay liner, it is anticipated that coal liquefaction dissolver vessels will be fabricated similarly. In the event the stainless steel liner is breached, the ferritic 2-1/4 Cr-1Mo steel shell will be exposed to the coal liquefaction environment. Consequently, the objective of this investigation is to evaluate the mechanical property integrity of liquefaction process plant dissolver vessel materials, especially 2-1/4 Cr-1Mo steel. During the past year, several aspects of the 2-1/4 Cr-1Mo steel evaluation have been in progress: these include electron-microprobe analysis of scales formed in the slurry-hydrogen environment, scaling rate measurements, low cycle fatigue of compact tension fracture mechanics specimens (CTS) at ambient temperature, crack growth of bolt-loaded CTS in slurry-hydrogen, calculation of phase stability diagrams relevant to coal liquefaction conditions, and hydrogen attack evaluations. Results to date are reported.
Research Organization:
Ames Lab., IA (USA)
DOE Contract Number:
W-7405-ENG-82
OSTI ID:
6528579
Report Number(s):
IS-M-322; CONF-801079-3; ON: DE81023615
Country of Publication:
United States
Language:
English