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U.S. Department of Energy
Office of Scientific and Technical Information

Process for producing a powder of perovskite-type double oxide

Patent ·
OSTI ID:6352461

A process is described for producing a powder of perovskite-type double oxide represented by the formula ABO[sub 3], wherein A represents a metal material which is at least one member selected from the group consisting of Pb and a combination of Pb and at least one element selected form among Ba, Sr, Ca, La, and Li, B represents a metal material selected from the group consisting of a combination of Nb and at least one additional element selected from among Zn, Mg, Zr, Ti, Ni, Fe, W, Co, and Mn, and 0 represents oxygen, comprising the steps of: forming a homogeneous solution containing metal material B, by adding a solution containing a metal ion of Nb to a solution containing a metal ion of at least on of said additional element thereby preparing a homogeneous containing metal material B; reacting a solution containing a metal material A, and an aqueous solution of alkaline metal in a reaction vessel, thereby precipitating the hydroxide of metal material A; adding said homogeneous solution containing metal material B to said hydroxide precipitate of metal material A in a reaction vessel, thereby precipitating the hydroxide of metal material B in the obtained mixture; reacting hydrothermally the obtained mixture in the reaction vessel; filtering the reacted mixture; cleaning and drying the filtered precipitate; and heat-treating and pulverizing the dried precipitate.

Assignee:
IMS; EDB-93-106277
Patent Number(s):
A; US 5229101
Application Number:
PPN: US 7-638960
OSTI ID:
6352461
Country of Publication:
United States
Language:
English