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Syntheses and magnetic properties of Tb{sub 3}Fe{sub 29{minus}x}Cr{sub x} compounds

Journal Article · · Physical Review, B: Condensed Matter
; ; ;  [1];  [2]
  1. State Key Laboratory for Magnetism, Institute of Physics, Chinese Academy of Sciences, P.O. Box 603, Beijing 100080, Peoples Republic of (China)
  2. Department of Physics, Beijing Normal University, Beijing 100875, Peoples Republic of (China)

Compounds with composition Tb{sub 3}Fe{sub 29{minus}x}Cr{sub x} (x=1.0, 1.5, 2.0, and 3.0) have been synthesized successfully. The lattice parameters, the unit cell volume, the density, and the atomic positions of these compounds have been derived from x-ray diffraction patterns. The Curie temperature, the saturation magnetization, and the anisotropy field at 4.2 K and room temperature of these compounds are also obtained. The saturation magnetization of Tb{sub 3}Fe{sub 29{minus}x}Cr{sub x} decreases but the anisotropy field increases linearly with increasing Cr concentration at 4.2 K and room temperature. A spin reorientation of the easy-magnetization direction occurs at around 180 K and a first-order magnetization process is observed in magnetic fields in the range between 2.3 and 1.6 T at room temperature for the Tb{sub 3}Fe{sub 29{minus}x}Cr{sub x} compounds. The relationship between the hexagonal R{sub 2}T{sub 17} (2:17H), tetragonal RT{sub 12{minus}x}T{sub x}{sup {prime}} (1:12), and monoclinic R{sub 3}T{sub 29{minus}x}T{sub x}{sup {prime}} (3:29) structures are obtained through the matrix transformation of reciprocal vectors in a Cartesian coordinate system. Based on the experimental results of the saturation magnetization and the average hyperfine field of Tb{sub 3}Fe{sub 29{minus}x}Cr{sub x} compounds, the average Fe atomic magnetic moments in the range 0{le}x{le}3 can be expressed as an empirical formula: M{sub Fe}=M{sub Fe}(1){minus}x[M{sub Fe}(1){minus}M{sub Fe}(2)]/X{sub max} where M{sub Fe}(1) is the iron moment in 2:17 compounds, M{sub Fe}(2) is the iron moment in 1:12 compounds and X{sub max}=3 is the highest Cr concentration included. {copyright} {ital 1997} {ital The American Physical Society}

OSTI ID:
632634
Journal Information:
Physical Review, B: Condensed Matter, Journal Name: Physical Review, B: Condensed Matter Journal Issue: 14 Vol. 56; ISSN 0163-1829; ISSN PRBMDO
Country of Publication:
United States
Language:
English