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Creep-rupture behavior of iron superalloys in high-pressure hydrogen

Technical Report ·
OSTI ID:6324730

The creep-rupture behavior of a newly developed cast alloy NASAUT 4G-A1 with 15% Cr, 15% Mn, and 1.5% C was evaluated in 15 MPa H/sub 2/ at 775/sup 0/C and 825/sup 0/C; the alloy is intended for automotive Stirling heater head application. Rupture life, minimum creep rate, and time to 1% strain data were analyzed. The 3500-h mean rupture stress at 775/sup 0/C is 140 MPa, exceeding the design stress of 119 MPa. However, significant data scatter caused the 90% confidence level lower limit of the mean stress to be 94.3 MPa, falling below the 119 MPa design stress level. NASAUT 4G-A1 3500-h rupture-life mean stress exceeds the XF-818 values but is lower than SA-F11, HS-31, and CRM-6D (aged). The predicted mean stress to 1% creep in 3500 h was 57.8 MPa and had a very wide scatter indicating a lack of reproducibility in the alloy structure. For a cast alloy, NASAUT 4G-A1 indicated significant ductility with maximum elongation in the range of 6.0 to 13.6% at 775/sup 0/C. Hydrogen did not seem to affect the stable carbides though some methane was noted in the chamber gas. The microstructure contained some voids, pores, inclusions, and interdendritic separations. The structure consisted of an austenitic phase with two different carbides and was not affected by heat treatment.

Research Organization:
IIT Research Inst., Chicago, IL (USA)
DOE Contract Number:
AI01-77CS51040
OSTI ID:
6324730
Report Number(s):
DOE/NASA-0363-1; NASA-CR-175027; ON: DE86005013
Country of Publication:
United States
Language:
English