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Title: Fabrication of hollow silica aerogel spheres by a droplet generation method and sol--gel processing

Journal Article · · J. Vac. Sci. Technol., A; (United States)
DOI:https://doi.org/10.1116/1.576250· OSTI ID:6316914

A system was designed to produce hollow silica aerogel spheres by combining a droplet generation method with sol--gel processing. Simultaneous passage of an alkoxide solution and a fill gas, through a dual-nozzle system, formed a continuous stream of hollow droplets in the fluid state. The spherical droplets were levitated in a basic atmosphere containing ammonia which converted the sol into a rigid gel state. Supercritical drying was used for the elimination of residual solvents without shrinkage and cracking.

Research Organization:
Fusion Technology Laboratory, University of Illinois, Urbana, Illinois 61801
OSTI ID:
6316914
Journal Information:
J. Vac. Sci. Technol., A; (United States), Vol. 7:3
Country of Publication:
United States
Language:
English