Synthesis of nitramines. Final report
Technical Report
·
OSTI ID:6286303
Using known procedures, the following nitramines have been prepared: 20 g of 1,5-dinitro-3,7-endomethylene-1,3,5,7-tetrazacyclooctane; 5 g of 1-aceto-3,5,7-trinitro-1,3,5,7-tetrazacyclooctane; 9.5 g of 1,9-dinitroxy-2,4,6,8-tetranitrazanonane; 46 g of 1,9-diacetoxy-2,4,6,8-tetranitrazanonane; 7.3 g of 1,7-dinitroxy-2,4,6-trinitrazaheptane; and 42 g of 1,7-diacetoxy-2,4,6-trinitrazaheptane. The nitramines were purified to a constant melting point by repeated recrystallization. The purity and identity were confirmed by elemental analyses.
- Research Organization:
- Stanford Research Inst., Menlo Park, CA (USA)
- DOE Contract Number:
- AM03-76SF00115
- OSTI ID:
- 6286303
- Report Number(s):
- DOE/SF/00115-T8; ON: DE81026136
- Country of Publication:
- United States
- Language:
- English
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Related Subjects
37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CHEMISTRY
400301* -- Organic Chemistry-- Chemical & Physicochemical Properties-- (-1987)
AMINES
CARBON
CHEMICAL ANALYSIS
DATA
ELEMENTS
EXPERIMENTAL DATA
HYDROGEN
INFORMATION
MELTING POINTS
NITRO COMPOUNDS
NITROGEN
NONMETALS
NUMERICAL DATA
ORGANIC COMPOUNDS
ORGANIC NITROGEN COMPOUNDS
PHYSICAL PROPERTIES
PURIFICATION
QUANTITATIVE CHEMICAL ANALYSIS
RECRYSTALLIZATION
SYNTHESIS
THERMODYNAMIC PROPERTIES
TRANSITION TEMPERATURE
400301* -- Organic Chemistry-- Chemical & Physicochemical Properties-- (-1987)
AMINES
CARBON
CHEMICAL ANALYSIS
DATA
ELEMENTS
EXPERIMENTAL DATA
HYDROGEN
INFORMATION
MELTING POINTS
NITRO COMPOUNDS
NITROGEN
NONMETALS
NUMERICAL DATA
ORGANIC COMPOUNDS
ORGANIC NITROGEN COMPOUNDS
PHYSICAL PROPERTIES
PURIFICATION
QUANTITATIVE CHEMICAL ANALYSIS
RECRYSTALLIZATION
SYNTHESIS
THERMODYNAMIC PROPERTIES
TRANSITION TEMPERATURE