Method of reclaiming water and coal from coal treatment underflow by two-stage separation of solids

Patent · Tue Oct 16 04:00:00 EDT 1984

OSTI ID:6252129

Messer, L

Both water and carbonaceous material are reclaimed from an aqueous slurry of particles of coal that contains both carbonaceous and non-carbonaceous materials, the slurry being comprised of at least 60% water by weight. Preferably, the geometric mean particle size of the coal particles in the aqueous slurry is less than 150 microns. Preferably, the processed aqueous slurry is formed by mixing a low solids aqueous slurry of coal and ash fines from a coal washer with a high solids aqueous slurry of coal and ash fines from a settling pond. A fluid that is in a free-flowing liquid state at temperatures below 80/sup 0/C. and, preferably, at temperatures below 20/sup 0/C., and that is lyophobic to the water and the non-carbonaceous particles of the coal, and lyophillic to the carbonaceous fine particles of the coal is added to the aqueous slurry to form a first mixture in which less than 20% by weight of the fluid and the carbonaceous and non-carbonaceous coal particles is fluid. The first mixture is then agitated to preferentially agglomerate the carbonaceous particles to form carbonaceous agglomerates while the non-carbonaceous particles remain substantially dispersed in the slurry. The carbonaceous agglomerates are separated from the mixture to form a substantially non-carbonaceous aqueous slurry. A preferably high molecular weight flocculant that is lyophobic to water and lyophilic to non-carbonaceous material is thereafter added to the non-carbonaceous aqueous slurry to form a second mixture, and flocculated solids precipitated from the second mixture to form water and precipitate from the second mixture. Flocculated solids are then separated from the precipitate to provide a substantially solids-free aqueous solution.

• Assignee: American Minechem Corporation
• Patent Number(s): US 4477353
• OSTI ID: 6252129
• Country of Publication: United States
• Language: English

Related Subjects

01 COAL, LIGNITE, AND PEAT
013000* -- Coal
Lignite
& Peat-- Transport
Handling
& Storage
ADDITIVES
CARBONACEOUS MATERIALS
COAL
COAL PREPARATION
COAL PREPARATION PLANTS
COPRECIPITATION
DISPERSIONS
ENERGY SOURCES
FLOCCULATION
FOSSIL FUELS
FUEL SLURRIES
FUELS
HYDROGEN COMPOUNDS
INDUSTRIAL PLANTS
LYOPHILIZATION
MANAGEMENT
MATERIALS
MATERIALS RECOVERY
MIXTURES
OXYGEN COMPOUNDS
PARTICLE SIZE
PRECIPITATION
PROCESSING
RECOVERY
SEPARATION PROCESSES
SIZE
SLURRIES
SUSPENSIONS
WASTE MANAGEMENT
WASTE PROCESSING
WATER