Synthesis of three ((trifluoroethyl)amino)pyridines
Journal Article
·
· J. Chem. Eng. Data; (United States)
The synthesis of o-, m, and p-((trifluoroethyl)amino)pyridine by diborane/tetrahydrofuran reduction of the corresponding trifluoroacetamide is described. The yields were 52%, 83%, and 76%, respectively. The synthesis, in 53% yield, of 2,2,2-trifluoro-N-(4-pyridyl)acetamide is also described.
- Research Organization:
- Lawrence Livermore National Lab., CA
- DOE Contract Number:
- W-7405-ENG-48
- OSTI ID:
- 6226286
- Journal Information:
- J. Chem. Eng. Data; (United States), Journal Name: J. Chem. Eng. Data; (United States) Vol. 26:2; ISSN JCEAA
- Country of Publication:
- United States
- Language:
- English
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Related Subjects
37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CHEMISTRY
400301* -- Organic Chemistry-- Chemical & Physicochemical Properties-- (-1987)
AMINES
AZINES
CHEMICAL PREPARATION
CHEMICAL REACTION YIELD
HETEROCYCLIC COMPOUNDS
ORGANIC COMPOUNDS
ORGANIC FLUORINE COMPOUNDS
ORGANIC HALOGEN COMPOUNDS
ORGANIC NITROGEN COMPOUNDS
PYRIDINES
SYNTHESIS
YIELDS
400301* -- Organic Chemistry-- Chemical & Physicochemical Properties-- (-1987)
AMINES
AZINES
CHEMICAL PREPARATION
CHEMICAL REACTION YIELD
HETEROCYCLIC COMPOUNDS
ORGANIC COMPOUNDS
ORGANIC FLUORINE COMPOUNDS
ORGANIC HALOGEN COMPOUNDS
ORGANIC NITROGEN COMPOUNDS
PYRIDINES
SYNTHESIS
YIELDS