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Superconducting and normal state properties of hexagonal tungsten bronzes RhWO/sub 3/, Rh/sub 2/, WO/sub 3/ and K/sub x/ WO/sub 3/

Thesis/Dissertation ·
OSTI ID:6167681

Measurements of the resistivity rho, Hall voltage V/sub H/, Seebeck coefficient S, superconducting transition temperature T/sub c/, and the superconducting upper critial field H/sub c2/ were obtained for single crystals of K/sub x/ WO/sub 3/(0.18 < x < 0.33). Concentration-dependent and temperature-dependent transitions were observed similar to those reported for the Rb-HTB. Associated with the temperature-dependent phase transitions are anomalies in the resistivity, Hall coefficient and Seebeck coefficient. The concentration dependence of the onset temperatures of the anomalies showed a maximum near x = 0.25 indicating a phase transition with concentration. Associated with this transition are a suppressed superconducting T/sub c/, a sharp drop in the residual resistivity, a rise in the residual resistance ratio, and a break in the slope of the Seebeck coefficient with temperature. The angular variation of the critical field has been measured for the K-HTB and for hexagonal Rb/sub x/Cs/sub y/WO/sub 3/ with x + y = 0.24. A 6-fold anisotropy in H/sub c2/ was observed in the basal plane. The magnitude of H/sub c2/ was observed to depend on both the concentration and the size of the insertion ion. The resistivity and superconducting T/sub c/ measurements were also obtained on a single-crystals of Rb/sub x/Cs/sub y/WO/sub 3/. The temperature-dependent anomaly was suppressed with relatively small amounts of Cs content. T/sub c/ increased with increasing Cs content for total concentrations x + y = 0.24 and remained nearly constant for x + y = 0.28. The concentration dependence of the superconducting properties of Rb/sub x/WO/sub 3/ was analyzed using two methods.

Research Organization:
Florida State Univ., Tallahassee (USA)
OSTI ID:
6167681
Country of Publication:
United States
Language:
English