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U.S. Department of Energy
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Dewatering studies of fine clean coal

Technical Report ·
OSTI ID:6133186
 [1]
  1. Kentucky Univ., Lexington, KY (USA). Center for Applied Energy Research
Physical cleaning of ultra-fine coal using advanced froth flotation technique provides a low ash product; however, the amount of water associated with clean coal is high. Economic removal of water from the froth will be important for commercial applicability of the novel processes. The main objective of the present research program is to study and understand dewatering characteristics of ultra-fine clean coal and to develop process parameters to effectively reduce the moisture to less than 20 percent in the clean coal product. The research approach utilizes synergistic effect of metal ions and surfactant to lower the moisture of clean coal using conventional vacuum dewatering technique. During this contract period clean coal product obtained using the advanced Ken-Flote column was characterized. The average particle size of the clean coal was 21 microns and contained about 8 percent ash. The electrokinetic studies conducted on the coal before and after flotation shows a strong adsorption of fuel oil on the coal surface. Adsorption of Cu(II) metal ions and a cationic surfactant lowered the zeta potential to zero, depending on the pH of the suspension. Dewatering of clean coal froth without addition of any reagent provided 35 percent moisture cake; addition of 2.5 lb/ton of fuel oil reduced moisture to 30 percent. Efforts are in progress to understand adsorption phenomena of the reagents, contact angle studies and micrographic analysis of the filter cake. From these data, optimum process conditions will be identified to obtain a filter cake containing less than 20 percent moisture. 10 figs., 1 tab.
Research Organization:
Illinois Dept. of Energy and Natural Resources, Springfield, IL (USA)
Sponsoring Organization:
DOE; USDOE, Washington, DC (USA)
DOE Contract Number:
FG22-90PC90176
OSTI ID:
6133186
Report Number(s):
DOE/PC/90176-T16; ON: DE91010498
Country of Publication:
United States
Language:
English