Dewaxing by a combination centrifuge/catalytic process including solvent deoiling
Patent
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OSTI ID:6092153
A hydrocarbon dewaxing process comprising the steps of: (a) chilling the waxy hydrocarbon feed to be dewaxed in the absence of solvent to crystallize a portion of the hard wax; (b) introducing the hydrocarbon feed to be dewaxed into a centrifuge; (c) centrifuging the solvent free hydrocarbon feed thereby generating two streams, stream (I) comprising a major portion of oil with a minor portion of entrained wax, stream (II) comprising a major portion of wax with a minor portion of entrained oil; (d) adding a dewaxing solvent to stream (II) generating a slurry A; (e) feeding slurry A to a centrifuge thereby separating slurry A into an oil-solvent stream (III) and a wax-solvent stream (IV); (f) passing the oil-solvent stream (III) to a membrane separation unit wherein the stream is separated into a recycle solvent stream and an oil-solvent stream of reduced solvent content (stream V); (g) passing oil-solvent stream (V) to an oil recovery unit wherein the stream is separated into a recycle solvent stream and an oil stream (VI); (h) passing the wax-solvent stream (IV) of step (e) to a wax recovery unit wherein the stream is separated into a recycle solvent stream and a recovered wax product stream; (i) combining wax-oil stream (I) of step (c) with oil stream (VI) of step (g) and passing the combined stream to a catalytic dewaxing unit wherein the combined waxy oil stream, in the presence of hydrogen, is contacted with a catalyst and has its wax content reduced, thereby generating a dewaxed oil product stream.
- Assignee:
- Exxon Research and Engineering Co.
- Patent Number(s):
- US 4477333
- OSTI ID:
- 6092153
- Country of Publication:
- United States
- Language:
- English
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